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Beilstein J. Org. Chem. 2022, 18, 182–189, doi:10.3762/bjoc.18.20
Graphical Abstract
Scheme 1: Examples of mechanochemical reactions using NFSI.
Scheme 2: Mechanochemical fluorination of arenes 1 with NFSI. (a) Product distributions and reaction conditio...
Figure 1: Time-resolved 2D plots of the mechanochemical reaction of: (a) 1c (0.59 mmol), NFSI (1.0 equiv), an...
Scheme 3: (a–f) Reactions of substrates 3 with NFSI. Reaction conditions: Substrates 3 (0.734 mmol) were mill...
Scheme 4: Regioselective C-3 mechanochemical amidation of 5 with NFSI.